Combi Flash 7650 Series Manual de usuario descargar pdf (Pagina 68)

CombiFlash Torrent® User Manual

3-6

c. Agitate the solvent for a moment to allow the sample to

adsorb to the silica.

d. Remove the solvent with a suitable method, such as

rotary evaporation. Alternatively, you can dry the

prepared cartridge after step 5 by drawing the solvent

out using a vacuum or using the Torrent’s air purge.

3. Load the media and sample mixture into the cartridge. Tap

the cartridge on the benchtop to settle the mixture.

4. Place a frit on the top of the cartridge. Force the frit down

against the mixture using the plastic plunger.

5. Wipe away any residual powder inside the neck and top

rim of the cartridge.

Note

You can remove solvent from a prepared cartridge by attaching the

cartridge cap and manually purging (TOOLS>MANUAL CONTROL)

the cartridge with air.

Note

Empty solid sample cartridges also allow a variety of adsorbents,

such as diatomaceous earth, boiling chips, cotton balls, or paper

wipes. Even with alternative adsorbents, always use top and

bottom frits to prevent fluid path problems.

After you have prepared the pre-filled or empty cartridge,

place the solid sample cartridge on the system:

1. Attach the desired adjustable cartridge cap:

• 60-5237-048, fits 12 and 20 gram solid load

cartridges.

• 60-5237-044, fits 32 and 65 gram solid load

cartridges.

• 60-5247-008, fits 125 and 260 gram solid load

cartridges.

• 60-5247-009, fits 750 gram solid load cartridges.

2. Press the lever on the side of the cap and fully extend the

plunger (Figure 3-3).

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Combi Flash 7650 Series Manual de usuario Pagina 68