Combi Flash 7650 Series Manual de usuario Pagina 57
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Section 2 Preparation
2-37
Note
When pumping solvents the first time, inspect the solvent and
waste connections to the system. If any leaks are observed, click
the STOP button. Correct the leak by tightening the fitting an
additional
1
4 turn, and then restart the pump by touching the
PRIME B button.
7. After at least 400 mL of solvent has been pumped, touch
the S
TOP button.
8. Touch the P
RIME A button. The solvent pump will start.
Inspect the solvent and waste lines and correct leaks if
necessary.
9. After at least 400 mL of solvent has been pumped, touch
the S
TOP button.
10.Close the Manual Control window.
11.After the pressure gauge on the touch screen has returned
to 0 psi, remove the column bypass tube and disconnect the
solid load cartridge tubing from the Sample Injection Port.
The column bypass tube should be drained and returned to
the accessory kit.
Note
If using the optional Sample Load Pump, purge the pump with at
least 20 mL of Solvent A and run the pump dry.
After purging the lines, the system is ready for the optional
system verification (Section 2.15) or operation (Section 3).
2.15 System Verification with Test Mix B
It is recommended that the system operation be verified. To do
so, perform a purification run using the supplied test mix vial.
1. Connect the Liquid Injection Accessory (60-5244-059) from
the accessory kit (60-5249-002) to the Sample Injection
Port.
2. Load a 330 gram column (69-2203-330) on the Torrent.
Rotate the column so the label faces the RFID antenna.
- CombiFlash Tor re n t 1
- User Manual 1
- 3. Operation 4
- 4. User Help Reference 4
- 5. Remote Interfaces 5
- 6. Maintenance 6
- 1.3 Operating Overview 9
- 1.4 Specifications 10
- Section 1 Introduction 11
- 1.6 Safety 15
- Warnings and Cautions 18
- Symboles de sécurité 18
- Advertencias y Precauciones 19
- 2.2 Instrument Location 22
- 2.3 Connect Power 22
- NSTALL OPTIONAL EQUIPMENT 23
- 2.5 Position the Torrent 24
- 2.6 Connect Solvent Lines 25
- (Solvent B) 26
- 2 turn using a wrench 27
- 8-inch fittings from the 28
- 2.8 Optional External Gas 31
- Waste (NO) 33
- In (Common) 33
- Drop Former (NC) 33
- ETWORK CONFIGURATION 34
- Section 2 Preparation 35
- From top of diverter valve 42
- Connect ELSD 43
- Standoffs (place over 45
- Disconnect 46
- 2.11 Grounding 48
- 2.12 Turn on Power 48
- 2.13 Configure the Torrent 48
- B priming pump 50
- 2.13.2 User Preferences 51
- EMOTE INTERFACES. Do not 52
- RIME B button 57
- Section 3 Operation 65
- 3.2 Sample Preparation 66
- 3.2.2 Solid Samples 67
- OOLS>MANUAL CONTROL) 68
- 4 turn to seal the fittings 71
- 3.4 Start a Default Method 72
- 3.4.1 Syringe Injection 74
- 3.5 During the Run 77
- Section 4 User Help Reference 81
- 4.1.2 Method File 82
- 4.2 PeakTrak Menu Options 83
- 4.2.1 File 84
- 4.2.1.1 New 84
- 4.2.1.2 Open 84
- 4.2.1.3 Manage Files 84
- 4.2.1.4 Set Data Path… 84
- [4.2.3.5]” command instead 85
- [4.3.5] window. From 85
- [4.2.1.9] menu command 86
- [4.3.7] window 87
- [4.3.8] 87
- [4.3.9] 87
- 4.2.3.4 Auto Zero 88
- 4.2.3.5 Edit defaults 88
- 4.2.3.6 Configuration 88
- 4.2.3.7 Set Password 88
- 4.2.3.8 User Management 88
- 4.3 PeakTrak Windows 90
- 4.3.1.1 Gradient Plot 91
- 4.3.1.2 Run Settings 91
- 4.3.1.5 Peak Collection Data 94
- 4.3.2 Method Editor 95
- 4.3.2.1 Button bar 95
- [4.3.10] settings 96
- [ON-LINE]. The 97
- [4.3.10] 98
- [4.4.5] 98
- 4.3.2.5 Peak Collection 99
- 4.3.2.6 Peak Detection 100
- 4.3.3 Gradient Optimizer 101
- [4.2.1.2] and SAVE 102
- [4.2.1.2] 103
- [4.2.3.1] menu command. The 104
- [4.2.3.3] from the 105
- [4.2.3.2] menu command. The 105
- [4.4.10] 106
- [4.2.3.3] menu 107
- [4.3.10.4] 107
- [ON-LINE] 107
- [4.3.11] 108
- [4.4.11] 108
- [4.3.2.5] settings on the 108
- ETWORK PRINTING feature 110
- 4.3.10.4 Fraction Collector 111
- 4.3.11 Set Password 112
- 4.3.12 User Management 113
- ON-LINE]) 114
- 4.4.2 Editing a method 117
- [4.4.5] topic for more 118
- [4.3.10] window 118
- [ON-LINE] for actual 119
- [4.2.1.9] 122
- [4.3.5] 123
- [4.2.3.5] menu command 123
- [4.4.2] 123
- [4.3.1] and 124
- [4.3.2] window 125
- [4.3.3]). Note the 126
- [4.3.5] window is displayed 127
- [4.3.1] 127
- [4.3.10.2] settings 128
- [4.4.7] help topic 129
- [4.3.9] window by 130
- [ON-LINE] topic 131
- CombiFlash To r re n t 133
- 5.1.1 Network PC Access 134
- 5.1.2 Network Printing 134
- Section 5 Remote Interfaces 135
- 5.2 Direct Connection 136
- 5.2.2 Windows Vista Settings 138
- 5.2.3 Windows XP Settings 140
- 5.2.4 Windows 2000 Settings 142
- 5.3 Direct Printing 144
- 6.2 Preventive Maintenance 146
- 6.3 Cleaning 147
- 6.4 Tubing Inspection 148
- 6.5 Flow Cell Cleaning 148
- Section 6 Maintenance 149
- Solvent Description 153
- DECLARATION OF CONFORMITY 157
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