Combi Flash 7650 Series Manual de usuario descargar pdf (Pagina 58)

CombiFlash Torrent® User Manual

2-38

CAUTION

Pinch point. Your fingers or hands can be seriously

injured if you place them between the moving parts of

the Solid Load Cartridge Cap Mount or the Upper

Column Mount. Use care when installing solid load

cartridges or columns.

3. Ensure the Torrent automatically loads a default method

for the column. If not, use the touch screen to manually

select the RediSep column media and size.

4. Touch the M

ETHOD EDITOR menu option to open the

Method Editor window.

5. Touch the T

IME TO CV (Column Volume) button to display

the run time in column volumes.

6. In the Peak Collection section of the display, select the

EAKS option.

7. Touch the E

XIT button and select the YES option to save the

changes.

8. Touch the P

LAY button. This opens the Run Requirements

window.

a. Select L

IQUID for the Sample Loading Technique.

b. Select the Start Rack and Start Tube number for the

fraction collector. If using the Fractionation Valve, the

set of containers is considered a rack. The Start Tube

number identifies which of the six valve positions to

start from.

c. Review the Solvent Requirements and add solvent if

necessary.

d. Touch the OK button to begin column equilibration.

9. Prepare the Test Mix B vial (60-5244-109) by completely

dissolving the dry sample in 2 mL of ethyl acetate.

Note

The solution should be used within 24 hours or discarded.

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Combi Flash 7650 Series Manual de usuario Pagina 58