Combi Flash 7650 Series Manual de usuario Pagina 120
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CombiFlash Torrent® User Manual
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When using the All or Peaks options, you can specify the
maximum Peak and Non-peak volumes to be collected in the
tubes. Be sure to enter volumes less than the maximum tube
capacity. Different peak and non-peak tube volumes can be
used to conserve tubes when using the All peak collection
mode by collecting large volumes of non-peak fluid while
creating more, smaller fraction volumes of fluids of interest.
The Foxy fraction collector or Fractionation Valve will advance
to the next tube whenever a peak is detected. Also note that
the fraction collector or valve will advance to the next tube if a
new peak is detected before completing the last one
(sometimes called a double advance). Keep in mind that the
slope and threshold detection methods use algorithms
optimize the peak detection. For example, peak detection
includes a hysteresis to reduce the likelihood of multiple tube
advances that may occur if there is noise at the beginning or
tail end of a peak.
These actions may be overridden if Time Windows are active.
See the discussion on I
NITIAL WASTE & TIME WINDOWS.
Peak Detection This section of the window contains option
buttons to enable and disable various peak detection options.
When an option is enabled, the window also allows you to
modify the setting details for that peak detection option. All
enabled options will be displayed on the chromatogram.
Note: You can select up to two peak detection options
(excluding the External option). If using two options, such as
1 with 2, PeakTrak considers a peak to be present when
either option is true (a logical OR).
• 1 and 2 (wavelength 1 and 2) — Enable these
options to use and configure primary and secondary
wavelength detection. When enabled, type or select the
peak detection wavelength in nanometers, then click the
Details button to configure additional settings described
below.
• Slope Based — Select this option to enable
Slope-based peak detection. When enabled, peaks will
be recorded if the slope algorithm indicates a peak
within the Peak Width setting.
- CombiFlash Tor re n t 1
- User Manual 1
- 3. Operation 4
- 4. User Help Reference 4
- 5. Remote Interfaces 5
- 6. Maintenance 6
- 1.3 Operating Overview 9
- 1.4 Specifications 10
- Section 1 Introduction 11
- 1.6 Safety 15
- Warnings and Cautions 18
- Symboles de sécurité 18
- Advertencias y Precauciones 19
- 2.2 Instrument Location 22
- 2.3 Connect Power 22
- NSTALL OPTIONAL EQUIPMENT 23
- 2.5 Position the Torrent 24
- 2.6 Connect Solvent Lines 25
- (Solvent B) 26
- 2 turn using a wrench 27
- 8-inch fittings from the 28
- 2.8 Optional External Gas 31
- Waste (NO) 33
- In (Common) 33
- Drop Former (NC) 33
- ETWORK CONFIGURATION 34
- Section 2 Preparation 35
- From top of diverter valve 42
- Connect ELSD 43
- Standoffs (place over 45
- Disconnect 46
- 2.11 Grounding 48
- 2.12 Turn on Power 48
- 2.13 Configure the Torrent 48
- B priming pump 50
- 2.13.2 User Preferences 51
- EMOTE INTERFACES. Do not 52
- RIME B button 57
- Section 3 Operation 65
- 3.2 Sample Preparation 66
- 3.2.2 Solid Samples 67
- OOLS>MANUAL CONTROL) 68
- 4 turn to seal the fittings 71
- 3.4 Start a Default Method 72
- 3.4.1 Syringe Injection 74
- 3.5 During the Run 77
- Section 4 User Help Reference 81
- 4.1.2 Method File 82
- 4.2 PeakTrak Menu Options 83
- 4.2.1 File 84
- 4.2.1.1 New 84
- 4.2.1.2 Open 84
- 4.2.1.3 Manage Files 84
- 4.2.1.4 Set Data Path… 84
- [4.2.3.5]” command instead 85
- [4.3.5] window. From 85
- [4.2.1.9] menu command 86
- [4.3.7] window 87
- [4.3.8] 87
- [4.3.9] 87
- 4.2.3.4 Auto Zero 88
- 4.2.3.5 Edit defaults 88
- 4.2.3.6 Configuration 88
- 4.2.3.7 Set Password 88
- 4.2.3.8 User Management 88
- 4.3 PeakTrak Windows 90
- 4.3.1.1 Gradient Plot 91
- 4.3.1.2 Run Settings 91
- 4.3.1.5 Peak Collection Data 94
- 4.3.2 Method Editor 95
- 4.3.2.1 Button bar 95
- [4.3.10] settings 96
- [ON-LINE]. The 97
- [4.3.10] 98
- [4.4.5] 98
- 4.3.2.5 Peak Collection 99
- 4.3.2.6 Peak Detection 100
- 4.3.3 Gradient Optimizer 101
- [4.2.1.2] and SAVE 102
- [4.2.1.2] 103
- [4.2.3.1] menu command. The 104
- [4.2.3.3] from the 105
- [4.2.3.2] menu command. The 105
- [4.4.10] 106
- [4.2.3.3] menu 107
- [4.3.10.4] 107
- [ON-LINE] 107
- [4.3.11] 108
- [4.4.11] 108
- [4.3.2.5] settings on the 108
- ETWORK PRINTING feature 110
- 4.3.10.4 Fraction Collector 111
- 4.3.11 Set Password 112
- 4.3.12 User Management 113
- ON-LINE]) 114
- 4.4.2 Editing a method 117
- [4.4.5] topic for more 118
- [4.3.10] window 118
- [ON-LINE] for actual 119
- [4.2.1.9] 122
- [4.3.5] 123
- [4.2.3.5] menu command 123
- [4.4.2] 123
- [4.3.1] and 124
- [4.3.2] window 125
- [4.3.3]). Note the 126
- [4.3.5] window is displayed 127
- [4.3.1] 127
- [4.3.10.2] settings 128
- [4.4.7] help topic 129
- [4.3.9] window by 130
- [ON-LINE] topic 131
- CombiFlash To r re n t 133
- 5.1.1 Network PC Access 134
- 5.1.2 Network Printing 134
- Section 5 Remote Interfaces 135
- 5.2 Direct Connection 136
- 5.2.2 Windows Vista Settings 138
- 5.2.3 Windows XP Settings 140
- 5.2.4 Windows 2000 Settings 142
- 5.3 Direct Printing 144
- 6.2 Preventive Maintenance 146
- 6.3 Cleaning 147
- 6.4 Tubing Inspection 148
- 6.5 Flow Cell Cleaning 148
- Section 6 Maintenance 149
- Solvent Description 153
- DECLARATION OF CONFORMITY 157
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